Preparation of Highly Concentrated Silver Nanoparticles in Reverse Micelles of Sucrose Fatty Acid Esters through Solid-Liquid Extraction Method
نویسندگان
چکیده
Silver nanoparticles were synthesized in reverse micelles consisting of sucrose fatty acid esters by dissolving reactant powder in the water pool of reverse micelles through the solid-liquid extraction. Silver nanoparticles having various sizes and shapes were obtained at high concentration. The size of silver nanoparticles was controlled by reaction temperature. Moreover, the size of silver nanoparticles was dependent upon the average esterification degree of sucrose fatty acid esters forming reverse micelles. The wavelength in the peaks, which corresponded upon the localized surface plasmon resonance of resultant silver nanoparticles, was correlated with their sizes.
منابع مشابه
Evaluation of Factors Inf luencing Recovery of Herbicide 2,4-D from Drinking Water
Many modern analytical methods deal with the trace-level determination of compounds of interest in highly complex environmental samples by means of chromatographic techniques. The introduction of a “clean” sample into an analytical instrument can make analyses easier and prolongs the equipment life. The use of solid-phase extraction (SPE) has grown and is a fertile technique of sample prepa...
متن کاملMonitoring ester formation in grape juice fermentations using solid phase microextraction coupled with gas chromatography-mass spectrometry.
Volatile esters contribute important floral and fruity sensory properties to wine. Numerous factors influence the biosynthesis and hydrolysis of esters throughout yeast fermentation; however, methods to monitor the dynamic changes in ester production that occur during winemaking processes are limited. In this study, we showed that solid phase microextraction (SPME), a rapid, solventless samplin...
متن کاملPreparation of Sodium Dodecyl Sulfate Modified Pyrrolidine-1-dithiocarboxylic acid Ammonium Coated Magnetite Nanoparticles for Magnetic Solid Phase Extraction of Pb(II) from Water Samples
This paper describes the development of a procedure for Pb(II) ions removal from various water samples after magnetic solid phase extraction (MNPs) by magnetite nanoparticles (Fe3O4 NPs) modified with sodium dodecyl sulfate (SDS) and pyrrolidine-1-dithiocarboxylic acid ammonium (PDTCAA). The synthesis of Fe3O4 NPs was certified by characterization techniques including field emission scanning el...
متن کاملPreparation of Sodium Dodecyl Sulfate Modified Pyrrolidine-1-dithiocarboxylic acid Ammonium Coated Magnetite Nanoparticles for Magnetic Solid Phase Extraction of Pb(II) from Water Samples
This paper describes the development of a procedure for Pb(II) ions removal from various water samples after magnetic solid phase extraction (MNPs) by magnetite nanoparticles (Fe3O4 NPs) modified with sodium dodecyl sulfate (SDS) and pyrrolidine-1-dithiocarboxylic acid ammonium (PDTCAA). The synthesis of Fe3O4 NPs was certified by characterization techniques including field emission scanning el...
متن کاملA Novel Method for the Preparation of Silver Halide Nanoparticles from Their Bulk Solid Using Microemulsions
Nanoparticles of silver halides are widely used to study the quantum confinement effects in indirect band gap semiconductors [1]. These particles are typically prepared by carrying out a precipitation reaction in the water pools of w/o microemulsions, or reverse micelles, by mixing two identical microemulsions containing aqueous solutions of AgNO3 and KBr, or other halides [2]. The mixing of tw...
متن کامل